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Oxygen bomb calorimeter instrument in the ignition wire is easy to burn out but sample coal not burn what reason be
Oxygen bomb calorimeter instrument in the ignition wire is easy to burn out but sample coal not burn what reason be
Second, check the calorimeter oxygen bomb is sufficient oxygen?
Third, oxygen bomb is leaking (usually seal ring)
Fourth, samples (coal samples / standard sample / standard material, etc.) have been dry air? Wet and easy to burn is not enough, samples (coal samples / standard sample / standard material, etc.) after sampling directly with a drying oven drying!
Fifth, calorimetry (kcal / calorimeter instrument) oxygen bomb ignition wire (nichrome wire wire and sample \ combustion) (coal sample / standard / standard substances) contact? Need the ignition wire (nichrome wire burning \ \ complete contact samples)!
Sixth, the voltage is too high? High ignition oxygen bomb calorimeter (wire nichrome wire \ burning wire is easy to break).
Seventh, the sample (coal sample / standard / standard substances) probably because of low calorific value (this is rarely higher than 200 kcal, will be successful, if the sample (coal) / sample) to low calorific value of additives, such as benzoic acid mixed with a certain quality of the calorific value of combustibles.